MECHANICAL PROPERTIES OF ALUMINIUM METAL MATRIX COMPOSITES REINFORCED WITH MILLSCALE AND ALUMINA

Authors

  • Adeolu A. Adediran Materials Design and Structural Integrity Research Group, Department of Materials and Metallurgical Engineering, Federal University Oye Ekiti
  • Oreofeoluwa A. Mosadomi Materials Design and Structural Integrity Research Group, Department of Materials and Metallurgical Engineering, Federal University Oye Ekiti
  • Peter P. Ikubanni Department of Mechatronics Engineering, Bowen University, Iwo
  • Chioma I. Madueke Materials Design and Structural Integrity Research Group, Department of Materials and Metallurgical Engineering, Federal University Oye Ekiti
  • Reginald Umunakwe Materials Design and Structural Integrity Research Group, Department of Materials and Metallurgical Engineering, Federal University Oye Ekiti

DOI:

https://doi.org/10.59957/jctm.v61.i3.2026.14

Keywords:

aluminium matrix composite, millscale, alumina, mechanical properties, composite materials

Abstract

The present investigation examines the mechanical properties of aluminium metal matrix composites (AMCs) that are reinforced with millscale and alumina. The composite materials were produced through a stir casting technique and analysed for density, porosity, hardness, tensile strength, yield strength, specific strength, percentage elongation and fracture toughness. The microstructure of the produced composites and the fractured surfaces of the composites were examined using a scanning electron microscope (SEM). The findings demonstrate that the addition of millscale and alumina improves the mechanical properties of the composites. The mechanical testing reveals a gradual increase in tensile strength with a higher weight ratio of alumina, resulting in a maximum ultimate tensile
strength of 124.73 MPa for sample D. Moreover, hardness increases slightly with higher weight ratios of alumina, with sample D exhibiting the highest hardness value of 94.6 BHN. Fracture toughness varies with composition, and sample D displays a fracture toughness of 7.6 MPa m0.5. The incorporation of alumina enhances hardness, yield strength, and tensile strength. Whereas the presence of millscale leads to improved hardness and tensile strength. The incorporation of millscale and alumina markedly improves the specific strength of the composites. The analysis of the microstructure demonstrates the distribution and bonding properties of the reinforcement particles in the aluminium matrix. The findings indicate the potential of millscale and alumina as reinforcing materials for AMCs, providing a sustainable and cost-effective solution for diverse engineering applications. 

References

Adediran, A. A., Edoziuno, F. O., Adesina, O. S., Sodeinde, K. O., Ogunkola, A. B., Oyinloye, G. A., & Akinlabi, E. T. (2022). Mechanical characterization and numerical optimization of aluminium matrix hybrid composite. In Materials Science Forum (Vol. 1065, pp. 47-57). Trans Tech Publications Ltd.

Adediran, A., Alaneme, K., Oladele, I., Akinlabi, E., & Sánchez, J. (2021). Microstructural characteristics and mechanical behaviour of aluminium matrix composites reinforced with Si-based refractory compounds derived from rice husk. Cogent Engineering. https://doi.org/10.1080/23311916.2021.1897928

Adeleke, A.A., Ikubanni, P.P., Odusote, J.K., Olujimi, B.B., Okolie, J.A. (2023). Influence of sawdust ash on the microstructural and physicomechanical properties of stir-cast Al6063/SDA matrix composite. The Journal of Advanced Manufacturing Technology. 127, 2523–2536. https://doi.org/10.1007/s00170-023-11700-xAdesina, O. S., Akinwande, A. A., Adediran, A. A., Balogun, O. A., Sanyaolu, O. O., and Romanovski, V. (2023). Morphological evolution and strength performance of green-aluminium-7075 hybrid composites modeled by response surface analysis. Multiscale and Multidisciplinary Modeling, Experiments and Design, 1-33.

Alaneme, K. K., Akintunde, I. B., Olubambi, P. A., & Adewale, T. M. (2013). Fabrication characteristics and mechanical behaviour of rice husk ash–alumina reinforced Al-Mg-Si alloy matrix hybrid composites. Journal of Materials Research and Technology, 2(1), 60-67.

Alaneme, K. K., Mayokun, O., Bodunrin, M. O., Babalola, S. A., Adediran, A. A., & Olaleye, K. J. (2022). On the applicability of Cu–17Zn–7Al–0.3 Ni shape memory alloy particles as reinforcement in aluminium-based composites: Structural and mechanical behaviour considerations. Journal of the Mechanical Behaviour of Materials, 31(1), 663-672.

Alaneme, K., & Ajayi, O. (2017). Microstructure and mechanical behaviour of stir-cast Zn–27Al-based composites reinforced with rice husk ash, silicon carbide, and graphite. Journal of King Saud University-Engineering Sciences, 29(2), 172-177.

Alaneme, K., Okotete, E., Fajemisin, A., & Bodunrin, M. (2019). Applicability of metallic reinforcements for mechanical performance enhancement in metal matrix composites: A review. Arab Journal of Basic and Applied Sciences, 26(1), 311-330.

Anestiev, L., Lazarova, R., Petrov, P., Dyakova, V., & Stanev, L. (2021). On the strengthening and the strength-reducing mechanisms at aluminium matrix composites reinforced with nano-sized TiCN particulates. Philosophical Magazine, 101(2), 129-153.

Atuanya, C. U., Ibhadode, A. O. A., & Dagwa, I. M. (2012). Effects of breadfruit seed hull ash on the microstructures and properties of Al–Si–Fe alloy/breadfruit seed hull ash particulate composites. Results in Physics, 2, 142-149.

Babu, M. N., & Sasikala, G. (2020). Effect of temperature on the fatigue crack growth behaviour of SS316L (N). International Journal of Fatigue, 140, 105815.

Bagatini, M. C., Zymla, V., Osório, E., & Vilela, A. C. F. (2011). Characterization and reduction behaviour of mill scale. Isij International, 51(7), 1072-1079..

Balokhonov, R., Romanova, V., Zinovieva, O., & Zemlianov, A. (2022). Microstructure-based analysis of residual stress concentration and plastic strain localization followed by fracture in metal-matrix composites. Engineering Fracture Mechanics, 259, 108138.

Bannaravuri, P. K., & Birru, A. K. (2018). Strengthening of mechanical and tribological properties of Al-4.5% Cu matrix alloy with the addition of bamboo leaf ash. Results in Physics, 10, 360-373.

Bhoi, N. K., Singh, H., & Pratap, S. (2020). Developments in aluminium metal matrix composites reinforced by micro/nano particles–A review. Journal of Composite Materials, 54(6), 813-833.

Bugdayci, M., Alkan, M., Turan, A., & Yücel, O. (2018). Production of iron-based alloys from mill scale through metallothermic reduction. High Temperature Materials and Processes, 37(9-10), 889-898.

Chairi, M., El Bahaoui, J., Hanafi, I., Favaloro, F., Borsellino, C., & Di Bella, G. (2023). Finite element analysis of ceramic–composite structures for ballistic applications: Effect of ceramic thickness and cell structure. Advanced Engineering Materials, 25(24), 2301089.

Chen, L., Sun, Y., Li, L., & Ren, X. (2020). Microstructure evolution, mechanical properties, and strengthening mechanism of TiC-reinforced Inconel 625 nanocomposites fabricated by selective laser melting. Materials Science and Engineering: A, 792, 139655.

Damian, C. S., Devarajan, Y., & Jayabal, R. (2024). A comprehensive review of the resource efficiency and sustainability in biofuel production from industrial and agricultural waste. Journal of Material Cycles and Waste Management, 26(3), 1264-1276.

Deng, Y., Li, W., Shao, J., Zhang, X., Kou, H., Ma, J., & Wang, R. (2018). Modelling the temperature-dependent non-steady state first matrix cracking stress for fiber ceramic matrix composites. Journal of Alloys and Compounds, 740, 987-996.

Dieter, G. E. (2000). Mechanical behaviour under tensile and compressive loads. ASM Handbook, 8, 99-108.

Durowaye, S. I., Sekunowo, O. I., Lawal, A. I., & Ojo, O. E. (2017). Development and characterisation of iron millscale particle reinforced ceramic matrix composite. Journal of Taibah University for Science, 11(4), 634-644.

Edoziuno, F., Adediran, A., Odoni, B., Utu, O., & Olayanju, A. (2020). Physico-chemical and morphological evaluation of palm kernel shell particulate reinforced aluminium matrix composites. Materials Today: Proceedings. https://doi.org/10.1016/j.matpr.2020.03.641

Gebrehiwet, L., Abate, E., Negussie, Y., Teklehaymanot, T., & Abeselom, E. (2023). Application of composite materials in aerospace & automotive industry. International Journal of Advances in Engineering and Management (IJAEM, 5) (3), 697-723.

Halil, K., İsmail, O., Sibel, D., & Ramazan, Ç. (2019). Wear and mechanical properties of Al6061/SiC/B4C hybrid composites produced with powder metallurgy. Journal of Materials Research and Technology, 8(6), 5348-5361.

Hussain, L., Praveen, P., Ragavu, S., Pahwa, S., Jain, A., Anandhi, R. J., & Praveena, K. (2024). The development of composites materials: From conventional to innovative uses. In E3S Web of Conferences (Vol. 529, p. 01050). EDP Sciences.

Ikubanni, P.P., Oki, M. and Adeleke, A.A. (2020). A review of ceramic/bio-based hybrid reinforced aluminium matrix composites. Cogent Engineering, 7: 1727167, 1 – 19.

Ikubanni, P.P., Oki, M., Adeleke, A.A., and Omoniyi, P.O. (2021a). Synthesis, physico- mechanical, and microstructural characterization of Al6063/SiC/PKSA hybrid reinforced composites. Scientific Report, 11:14845; 1-13.

Ikubanni, P., Oki, M., Adeleke, A., Adediran, A., Agboola, O., Babayeju, O., & Omiogbemi, I. (2021b). Tribological and physical properties of hybrid reinforced aluminium matrix composites. Materials Today: Proceedings, 46, 5909–5913. https://doi.org/10.1016/j.matpr.2021.03.537

Ikubanni, P., Oki, M., Adeleke, A., Adesina, O., & Omoniyi, P. (2021c). Physico-tribological characteristics and wear mechanism of hybrid reinforced Al6063 matrix composites. Acta Metallurgica Slovaca, 24(7), 172-179.

Ikubanni, P.P., Oki, M., Adeleke, A.A., Adesina, O.S., Omoniyi, P.O., Akinlabi, E.T. (2022). Electrochemical studies of the corrosion behaviour of Al/SiC/PKSA hybrid composites in 3.5% NaCl solution. Journal of Composites Science, 6, 286.

Jjagwe, J., Olupot, P. W., & Carrara, S. (2023). Iron oxide nanoparticles/nanocomposites derived from steel and iron wastes for water treatment: A review. Journal of Environmental Management, 343, 118236.

Khaerudini, D. S., Chanif, I., Insiyanda, D. R., Destyorini, F., Alva, S., and Pramono, A. (2019). Preparation and characterization of mill scale industrial waste reduced by biomass-based carbon. Journal of Sustainable Metallurgy, 5, 510-518.

Kolapo, O. I., Olatise, A. D., Idowu, E. O., Omejalile, S. W., Abioye, T. E., & Kareem, B. (2024). Reinforcement of aluminium matrix composites with particulate agricultural waste derivatives for automotive applications: A review. Advances in Science and Technology, 154, 111-120.

Kumar, A., Singh, V. P., Singh, R. C., Chaudhary, R., Kumar, D., & Mourad, A. H. I. (2024). A review of aluminum metal matrix composites: Fabrication route, reinforcements, microstructural, mechanical, and corrosion properties. Journal of Materials Science, 59(7), 2644-2711.

Kumar, G. V., Panigrahy, P. P., Nithika, S., Pramod, R., & Rao, C. S. P. (2019). Assessment of mechanical and tribological characteristics of silicon nitride reinforced aluminium metal matrix composites. Composites Part B: Engineering, 175, 107138.

Liu, S., Li, C., Han, S., Deng, Y., & Zhang, X. (2015). Effect of natural aging on quench-induced inhomogeneity of microstructure and hardness in high-strength 7055 aluminium alloy. Journal of Alloys and Compounds, 625, 34-43.

Nath, S. K., & Das, U. K. (2006). Effect of microstructure and notches on the fracture toughness of medium carbon steel. Journal of Naval Architecture and Marine Engineering, 3(1), 15-22.

Parveez, B., Maleque, M. A., & Jamal, N. A. (2021). Influence of agro-based reinforcements on the properties of aluminium matrix composites: A systematic review. Journal of Materials Science, 56(29), 16195-16222.

Patel, M., Sahu, S. K., & Singh, M. K. (2020). Mechanical, tribological, and corrosion behaviour of aluminium alloys and particulate-reinforced aluminium or aluminium alloy metal matrix composites—A review. i-Manager’s Journal on Material Science, 8(2), 40.

Petrovic, J., Mladenovic, S., Markovic, I., and Dimitrijevic, S. (2022). Characterization of hybrid aluminum composites reinforced with Al2O3 particles and walnut-shell ash. Materiali in Tehnologije, 56(2), 115 – 122.

Prasad, D. S., Shoba, C., & Ramanaiah, N. (2014). Investigations on mechanical properties of aluminium hybrid composites. Journal of Materials Research and Technology, 3(1), 79-85.

Rajak, D. K., Pagar, D. D., Behera, A., & Menezes, P. L. (2022). Role of composite materials in automotive sector: Potential applications. Advances in Engine Tribology, 193-217.

Rajak, D. K., Pagar, D. D., Kumar, R., & Pruncu, C. I. (2019). Recent progress of reinforcement materials: A comprehensive overview of composite materials. Journal of Materials Research and Technology, 8(6), 6354-6374.

Sahu, M., Narasimhan, L., Raichur, A. M., Sover, A., Ciobanu, R. C., Lucanu, N., & Aradoaei, M. (2021). Improving fracture toughness of tetrafunctional epoxy with functionalized 2D molybdenum disulfide nanosheets. Polymers, 13(24), 4440.

Samal, P., Vundavilli, P. R., Meher, A., & Mahapatra, M. M. (2020). Recent progress in aluminum metal matrix composites: A review on processing, mechanical and wear properties. Journal of Manufacturing Processes, 59, 131-152.

Samuel, A. A., Adeleke, A. A., Ogedengbe, T., Aladejana, M., Ikubanni, P. P., Markus, S., ... & Labaran, A. D. (2023, November). The preparation techniques and application of aluminium metal matrix composites: A review. In 2023 2nd International Conference on Multidisciplinary Engineering and Applied Science (ICMEAS) (pp. 1-5). IEEE.

Sekunowo, O. I., Durowaye, S. I., & Lawal, G. I. (2019). Synthesis and characterisation of iron millscale particles reinforced ceramic matrix composite. Journal of King Saud University-Engineering Sciences, 31(1), 78-85.

Senthil, S., Raguraman, M., & Manalan, D. T. (2021). Manufacturing processes & recent applications of aluminium metal matrix composite materials: A review. Materials Today: Proceedings, 45, 5934-5938.

Singh, G., & Goyal, S. (2018). Microstructure and mechanical behaviour of AA6082-T6/SiC/B4C-based aluminium hybrid composites. Particulate Science and Technology, 36(2), 154-161.

Touzi, N., and Horchani-Naifer, K. (2023). A study on the preparation and characterization of pigment quality from mill scale steel wastes. Environmental Science and Pollution Research, 1-16.

Vieira, I., Vilarinho, I. S., Buruberri, L., Carneiro, J., & Seabra, M. P. (2024). Upcycling process of mill scale waste into high-value ceramic products. Ceramics International, 50(19), 36800-36810.

Wang, X., Gao, X., Zhang, Z., Cheng, L., Ma, H., & Yang, W. (2021). Advances in modifications and high-temperature applications of silicon carbide ceramic matrix composites in aerospace: A focused review. Journal of the European Ceramic Society, 41(9), 4671-4688.

Zelinskas, M. V. (2020). Improving the material properties of boron carbide through elemental inclusion (Doctoral dissertation, Monterey, CA; Naval Postgraduate School).

Downloads

Published

2026-05-01

Issue

Section

Articles